Thermal Desorption Spectroscopy (TDS) System for Hydrogen Analysis The "TDS System for Hydrogen Analysis" developed in collaboration with
NIMS (National Institute of Material Science) allows the user to measure/analyze
the mass of hydrogen contained in a steel piece. It is optimal for inspecting
the Hydrogen embrittlement of a steel piece or a product.
[ Summary ]
Allows quantitative measurement of Hydrogen inside a steel piece under atmospheric environment where corrosion takes place.
Allows mass measurement of Hydrogen desorbed from a heated steel piece using a high sensitive Q-MS.
Allows real-time desorption analysis.
Equipped with the standard Hydrogen leak, which allows the quantitative
measurement of hydrogen
Equipped with twin Turbo Molecular Pumps installed vertically, which allows residual Hydrogen inside the analysis chamber.
Equipped with a load-lock chamber, which helps to exhaust introduction of
a steel piece without exposing thermal resistant tube and analysis chamber
to the air.
Up toφ20mm x 50mm steel piece can be measured.
Equipped with a touch panel to control Pumps and Valves.
Leakage amount of H2 gas (high accuracy calibration at 3 points)
3.9 x 10-6atm · cc/s = approx. 75torr
1.9 x 10-5atm · cc/s = approx. 350torr
3.9 x 10-5atm · cc/s = approx. 760torr
Heating temp
RT~1000°C
Heating speed
50°C/hr~600°C/hr (Tolerance: +/-10°C)
Sample size
φ5mm x 10mm~φ20 x 50mm
Thermal resistant tube
φ32mm O.D. x 700mm (length)
Pump (load-lock chamber)
TMP (190L/sec w/ N2)
Sample introduction
Magnet feedthrough
Hydrogen computing software
- Displays spectra of desorbed hydrogen
- Calculates amount of desorbed Hydrogen based on the standard leak gas
value
- Calculates difference between Hydrogen background and desorbed Hydrogen
- Calculates desorbed Hydrogen weight in ppm
- Exports to Excel, etc.
